Methyl 4-(butyrylamino)-5-methyl-2-nitrobenzoate

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Methyl 4-(butyrylamino)-5-methyl-2-nitro­benzoate

The title compound, C(13)H(16)N(2)O(5), is useful as an inter-mediate in the field of agrochemicals. Intra-molecular C-H⋯O hydrogen bonds result in the formation of one six- and one five-membered nearly planar ring; the six-membered ring is also nearly coplanar with the adjacent benzene ring. In the crystal structure, inter-molecular C-H⋯O hydrogen bonds link the mol-ecules.

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The structure of the title compound, C(9)H(7)NO(6), is essentially planar [maximum deviation 0.284 (2)Å] except for the methyl H atoms. The crystal structure is stabilized by asymmetric O-H⋯O hydrogen bonds linking the hydrogen carboxyl-ates into pairs around the inversion centres. There is also π-π stacking of the benzene rings [centroid-centroid distance 3.6912 (12) Å].

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2-Methyl-5-[(3-methyl-4-nitro­benz­yl)sulfan­yl]-1,3,4-thia­diazole

The mol-ecule of the title thia-diazole derivative, C(11)H(11)N(3)O(2)S(2), has a butterfly-like structure and the whole mol-ecule is disordered with a site-occupancy ratio of 0.629 (4):0.371 (4). The mol-ecule is disordered in such a way that the 3-methyl-4-nitro-phenyl units of the major and minor components are approximately related by 180° rotation around the C-N bond axis. The dihedral ang...

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Methyl 5-chloro-2-(4-methyl­benzene­sulfonamido)­benzoate

In the title compound, C(15)H(14)ClNO(4)S, the benzene rings are oriented at a dihedral angle of 85.42 (1)°. An intra-molecular N-H⋯O hydrogen bond results in the formation of a five-membered ring and an intramolecular C-H⋯O inter-action also occurs.

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Methyl 4-amino-2-chloro­pyrimidine-5-carboxyl­ate

In the title compound, C6H6ClN3O2, all non-H atoms are approximately coplanar [maximum deviation = 0.012 (4) Å]; an intra-molecular N-H⋯O hydrogen bond occurs between the amino group and the carbonyl group. In the crystal, mol-ecules are linked by N-H⋯N hydrogen bonds into supra-molecular chains propagated along [101].

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2008

ISSN: 1600-5368

DOI: 10.1107/s1600536808005576